AgAuShield Plus

Column:Gold Protective Agent

Introduction

AgAuShield Plus is a water base solution which provides excellent protection for silver/silver alloy and gold/gold alloy surfaces. Tarnish resistance, anti-sulfide ability, and wear resistance are all improved dramatically after coating with the AgAuShield Plus protective agent.


Properties

● An ultra-thin protection film is formed after the workpieces are immersed in the AgAuShield Plus solution at 50ºC for 0.5 to 5.0 minutes.
● There is no negative effect on contact resistance and solderability.
● Wear resistance and tarnish resistance is improved dramatically.
● A short heat treatment of 200ºC will not adversely affect the protective properties of the ultra-thin film.
● Treatment with AgAuShield Plus does not cause water stains.
● AgAuShield Plus has a long bath life.


Composition of Plating Solution

AgAuShield Plus is dissolved in heated water (50ºC). It is then ready to use.


Operating Conditions

Parameter

Unit

Range

Optimal

AgAuShield Plus

mL/L

20 - 50

50

Temperature

45 - 55

55

Immersion Time

Minutes

0.5 - 4.0

2.0

Acidity of Solution

pH

9 - 11

9 - 11

Note: A longer immersion time will result in superior protection.


Solution Maintainance

DI water can be added to compensate for water evaporation. The reactive compound concentration needs to be maintained in 100%. Please see the “AgAuShield Plus Working Solution Maintenance and Addition” section for more details.


Preparation and Operation of Solution

Note: Before using AgAuShield Plus, shake the AgAuShield Plus for 1 minute at room temperature (below 25ºC).
1. Clean the container
2. Add 75% volume DI water and heat it to a temperature of 50 to 55ºC
3. Add AgAuShield Plus, and stir to form a homogeneous solution
4. Add water to the desired level, and stir the working solution for at least 1 minute
5. Adjust the working temperature to 50 to 55ºC


Equipment

Container: Stainless steel or PP
Ventilation: Required
Heat: PTFE


AgAuShield Plus Working Solution Maintenance and Addition

AgAuShield Plus

Working Solution Concentration (%)

Concentrated AgAuShield Plus

Addition (mL/L)

100

90

80

70

60

50

0

5

10

15

20

25

A. Note: Since the working solution is a gel solution, the particle size greatly affects the analysis results. This method is not very accurate for analyzing an aged working bath.
1. Procedure:
a) Put 20mL of the AgAuShield Plus working solution in a 250mL V flask
b) Add 20mL 0.1N Iodine
c) Stir for 10 minutes
d) Use 0.1N NaS2O3 to titrate to light yellow
e) Add 1mL 1% starch indicator
f) Continue to use 0.1N NaS2O3 to titrate to colorless (record the total V)
2. Calculation: AgAuShield Plus % = 400 - 20V

B. Troubleshooting

Issue

Causes

Solutions

Water stains

Workpiece parts are unclean

Ensure all parts are clean before applying AgAuShield Plus protective agent

Water rinse bath is contaminated

Use warm water or clean more thoroughly

Poor results on K2S 5% testing

Insufficent AgAuShield Plus

Adjust AgAuShield Plus to 100%

Incorrect temperature

Adjust the temperature to 50ºC

Insufficient immersion time

Extend the immersion time

Rinse water temperature is above 30℃

Decrease the rinse water temperature to 30℃


AgAuShield Plus MSDS English v1.pdf

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